مهندسی ساخت و تولید ایران

مهندسی ساخت و تولید ایران

بررسی تأثیر عملیات حرارتی آنیل بین پاسی و روانکار بر رفتار کشش سرد سوپر آلیاژ اینکونل X750 در فرایند مفتول‌کشی سرد

نوع مقاله : مقاله پژوهشی

نویسندگان
1 مجتمع دانشگاهی مهندسی مواد و فناوری‌های ساخت، دانشگاه صنعتی مالک اشتر، تهران، ایران
2 گروه مهندسی مواد، واحد علوم تحقیقات، دانشگاه آزاد اسلامی، تهران، ایران
10.22034/ijme.2025.509853.2058
چکیده
در تحقیق حاضر، تأثیر دما و زمان آنیل در محدوده‌ی دمایی 950 تا 1100 درجه سانتی‌گراد و مدت زمان‌های 1 تا 4 ساعت، بر ریزساختار و خواص مکانیکی مفتول تولید شده از جنس سوپر آلیاژ اینکونل X750 به روش کشش سرد توسط مطالعات ریزساختاری، بررسی های خواص مکانیکی و زبری سنجی بررسی ‌شده است. شمش اولیه توسط روش ذوب با قوس الکتریکی در خلأ ریخته‌گری شد، سپس قطر شمش از 25 میلی‌متر به 2 میلی‌متر توسط نورد شیاری داغ کاهش یافت. برای افزایش شکل پذیری، مفتول‌ها آنیل شدند. آنیل باعث کاهش استحکام کششی از 1600 به 800 مگاپاسکال و افزایش ازدیاد طول از 6 درصد به 70 درصد شد. با افزایش زمان آنیل اندازه دانه و ازدیاد طول افزایش و استحکام کاهش یافت. در فرایند مفتول کشی، مفتول اولیه در 6 مرحله آنیل و 11 پاس کشش سرد به قطر 1 میلی‌متر رسید. بهترین شرایط زمانی برای آنیل از بین زمان‌های 1 تا 4 ساعت، زمان 4 ساعت به دست آمد. بررسی‌های ریزساختاری، نشان داد که فرایند آنیل بین پاسی، باعث تبلور مجدد و بازیابی ساختار می‌شود و توان کار سختی افزایش‌یافته و پاس‌های بعدی مفتول‌کشی قابل انجام است. همچنین استفاده از روانکار حاوی MoS2، به علت کاهش اصطکاک باعث افزایش توانایی تغییر شکل سرد مفتول شد و تعداد مراحل آنیل را از 6 مرحله آنیل به 3 مرحله کاهش و استحکام کششی را از 900 به 1300 مگاپاسکال افزایش داد و زبری سطح از 3/8 به 6/2 میکرومتر کاهش یافت.
کلیدواژه‌ها

عنوان مقاله English

Investigation of the effect of inter-pass annealing heat treatment and lubricant on the cold drawing behavior of Inconel X750 superalloy during cold wire drawing process

نویسندگان English

Alireza Mirak 1
Amirsalar Dehghani 2
1 Faculty of Materials and Manufacturing Technologies, Malek Ashtar University of Technology, Tehran, Iran
2 Department of Materials Engineering, Science and Research Branch, Islamic Azad University, Tehran, Iran
چکیده English

In the present study, the effects of annealing temperature and time—within the temperature range of 950 to 1100 °C and durations from 1 to 4 hours—on the microstructure and mechanical properties of wire made from Inconel X-750 superalloy, produced by cold drawing, were investigated through microstructural analysis, mechanical testing, and surface roughness measurements. The initial ingot was cast using vacuum arc remelting, and its diameter was reduced from 25 mm to 2 mm through hot groove rolling. To enhance ductility, the wires underwent annealing. Annealing reduced the tensile strength from 1600 to 800 MPa and increased elongation from 6% to 70%. As annealing time increased, grain size and elongation increased, while tensile strength decreased. During the wire drawing process, the initial wire underwent six stages of annealing and eleven passes of cold drawing to reach a final diameter of 1 mm. Among the tested durations, the optimal annealing time was 4 hours. Microstructural examinations revealed that interpass annealing led to recrystallization and structural recovery, enhancing workability and allowing further drawing passes. Additionally, the use of a lubricant containing molybdenum disulfide reduced friction, thereby improving the cold formability of the wire, reducing the number of required annealing steps from six to three, increasing tensile strength from 900 MPa to 1300 MPa, and decreasing surface roughness from 3.8 to 2.6 µm.

کلیدواژه‌ها English

Inconel X750 Superalloy
Hot Caliber Rolling
Cold Wire Drawing
MoS2
[1] Rokhgireh H. Numerical Investigation of Creep Behavior Turbine blade made of Inconel 939 Superalloy with different Creep Models. Iranian Journal of Manufacturing Engineering. 2022 Mar 16;8(12):51-9. [In Persian]
[2] Buddaraju KM, Sastry GR, Kosaraju S. A review on turning of Inconel alloys. Materials Today: Proceedings. 2021 Jan 1;44:2645-52. doi: 10.1016/j.matpr.2020.12.673
[3] Marsh C, Depinoy S, Kaoumi D. Effect of heat treatment on the temperature dependence of the fracture behavior of X-750 alloy. Materials Science and Engineering: A. 2016 Nov 20;677:474-84. doi: 10.1016/j.msea.2016.09.081
[4] Chen MF, Cao SQ, Dong K. Study on the manufacturing process of large super alloy X-750 forgings for nuclear equipment. In International Conference on Nuclear Engineering 2022 Aug 8; 10.86458. doi: 10.1115/ICONE29-91791
[5] Changizian P, Yao Z, Xu S, Daymond MR, Griffiths M. Mechanical behavior of recrystallized and precipitation-hardened Inconel X-750 before and after helium-implantation and proton irradiation. Materials Characterization. 2023 Aug 1;202:112970. doi: 10.1016/j.matchar.2023.112970
[6] Judge CD, Bhakhri V, Jiao Z, Klassen RJ, Was G, Botton GA, Griffiths M. The effects of proton irradiation on the microstructural and mechanical property evolution of inconel X-750 with high concentrations of helium. Journal of Nuclear Materials. 2017 Aug 15;492:213-26. doi: 10.1016/j.jnucmat.2017.04.045
[7] Marzocca AL, Bozzano P, Nervi J. Microstructural characterization of Inconel X750 alloy used in reactors components. Microscopy and Microanalysis. 2020 Mar;26(S1):95-6. doi: 10.1017/S1431927620000707
[8] Ha JW, Seong BS, Jeong HW, Choi YS, Kang N. Effects of the aging temperature and stress relaxation conditions on γ′ precipitation in Inconel X-750. Journal of Nuclear Materials. 2015 Feb 1;457:362-8. doi: 10.1016/j.jnucmat.2014.11.093
[9] Kolagar AM. Additive manufacturing of nickel-based superalloy gas turbine components. Iranian Journal of Manufacturing Engineering. 2022 Sep 9(3):38-45. doi: 10.22034/IJME.2022.157668 [In Persian]
[10] Lothongkum G, Khuanheng W, Homkrajai W, Wangyao P. Effect of Pre-heat Treatments on Nano Gamma Precipitation and Mechanical Properties in Wrought Nickel Base Superalloy, X-750. Acta Metallurgica Slovaca. 2006;12(1):7-13.
[11] Del Valle JA, Picasso AC, Alvarez I, Romero R. Age-hardening behavior of Inconel X-750 superalloy. Scripta materialia. 1999 Jul 9;41(3):237-43. doi: 10.1016/S1359-6462(99)00151-7
[12] Sinha AK, Moore JJ. Study of precipitation and growth of γ′ and dislocation structure in Inconel X-750. Metallography. 1986 Feb 1;19(1):75-86. doi: 10.1016/0026-0800(86)90008-X
[13] Heydari B, Karimi Zarchi HR. Simultaneous optimization of surface roughness and material removal rate in dry turning of super alloy Inconel 600. Iranian Journal of Manufacturing Engineering. 2018 Nov 22;5(3):1-1. [In Persian]
[14] Ha JW, Seong BS, Jeong HW, Yoo YS, Choi YS, Kang N. Effect of cold drawing ratio on γ′ precipitation in Inconel X-750. Materials characterization. 2014 Oct 1;96:1-5. doi: 10.1016/j.matchar.2014.07.016
[15] de Souza GR, Gabriel SB, Dille J, dos Santos DS, de Almeida LH. Work hardening and aging contribution on the mechanical properties of X-750 nickel-based superalloy. Materials Science and Engineering: A. 2013 Mar 1;564:102-6. doi: 10.1016/j.msea.2012.10.095
[16] Prasad YV, Rao KP, Sasidhar S, editors. Hot working guide: a compendium of processing maps. 2nd ed. ASM international; 2015 Aug 1:490-493.
[17] Wang Y, Pan Q, Song Y, Li C, Li Z. Hot deformation and processing maps of X-750 nickel-based superalloy. Materials & Design. 2013 Oct 1;51:154-60. doi: 10.1016/j.matdes.2013.03.081
[18] Nowotnik A, Pędrak P, Sieniawski J, Góral M. Mechanical properties of hot deformed Inconel 718 and X750. Journal of Achievements in Materials and Manufacturing Engineering. 2012;50(2):74-80.
[19] Mahmoudi M, Aboutalebi MR, Salehi MT, Moshaver H, Ebrahimi GR, Vafaeenezhad H. Microstructure evolution, hot deformation behaviour and processing map of Inconel X-750 superalloy in sub-solvus and super-solvus temperature ranges. Journal of Materials Research and Technology. 2023 Sep 1;26:5594-616. doi: 10.1016/j.jmrt.2023.08.269
[20] Ballinger R, Elliott CS, Hwang IS, Prybylowski J. The effect of thermal treatment on the fracture properties of alloy X-750 in aqueous environments. Electric Power Research Inst., Palo Alto, CA (United States); Massachusetts Inst. of Tech., Cambridge, MA (United States); 1993 May 1.
[21] Arya A, Suwas S, Gérard C, Signor L, Thilly L, Chokshi AH. Strength and microstructure evolution in nickel during large strain wire drawing. Acta Materialia. 2021 Dec 1;221:117396. doi: 10.1016/j.actamat.2021.117396
[22] Kumar P, Philip JT, Wani MF, Rai H, Vashishtha H, Kuriachen B, Kumar D. Study of Tribological Properties of EN8 Steel against Inconel X-750 Alloy under Dry and Lubricated Conditions. Transactions of the Indian Institute of Metals. 2023 Sep;76(9):2353-61. doi: 10.1007/s12666-022-02787-z
[23] Changizian P, Yao Z, Daymond MR. Deformation mechanism characteristics in a Ni-based alloy X-750: Dislocation/precipitate interaction. Materials Characterization. 2021 Feb 1;172:110891. doi: 10.1016/j.matchar.2021.110891
[24] Del Valle JA, Picasso AC, Romero R. Work-hardening in Inconel X-750: study of stage II. Acta materialia. 1998 Mar 23;46(6):1981-8. doi: 10.1016/S1359-6454(97)00425-4
[25] Chen J, Jung P, Rödig M, Ullmaier H, Bauer GS. Ductility recovery in structural materials for spallation targets by post-irradiation annealing. Journal of nuclear materials. 2005 Aug 1;343(1-3):227-35. doi: 10.1016/j.jnucmat.2004.09.076