مهندسی ساخت و تولید ایران

مهندسی ساخت و تولید ایران

مطالعه رفتار خوردگی آلومینیوم آلیاژی 7075 فراوری شده با عملیات سایش مکانیکی سطح

نوع مقاله : مقاله پژوهشی

نویسندگان
گروه مهندسی مکانیک، دانشکده فنی و مهندسی، دانشگاه مراغه، مراغه، ایران
10.22034/ijme.2025.531053.2097
چکیده
اندازه‌ دانه به‌عنوان یکی از پارامترهای کلیدی ساختاری، نقش مهمی در تعیین رفتار مکانیکی و فیزیکی مواد فلزی ایفا می‌کند. عملیات ساچمه زنی با اعمال تنش‌های فشاری شدید به سطح ماده، اندازه‌دانه‌ها را به‌طور قابل ملاحظه‌ای در لایه سطحی کاهش می‌دهد؛ لذا، در این پژوهش، تأثیر عملیات سایش مکانیکی سطح بر رفتار مکانیکی و خوردگی آلومینیوم آلیاژی 7075 با تغییر مدت‌زمان ساچمه‌زنی و اندازه ساچمه مورد بررسی قرار گرفت. نتایج نشان داد که این فرایند، بدون توجه به پارامترهای اعمالی علاوه بر ریزدانه سازی از حدود ۱۵ میکرومتر به کمتر از ۳ میکرومتر، سختی نمونه‌ها را به طور قابل‌ملاحظه‌ای تا 50 درصد افزایش می‌دهد. افزایش مدت‌زمان ساچمه‌زنی و کاهش قطر ساچمه منجر به افزایش بیشتر سختی شد، به‌طوری‌که نمونه با ساچمه ۳ میلی‌متری و زمان ۱۰ دقیقه (نمونه 3-10) بیشترین سختی (۷۲ ویکرز، معادل ۵۰ درصد افزایش) را نشان داد. همچنین، عملیات ساچمه‌زنی موجب کاهش نرخ خوردگی پلاریزاسیون  نمونه‌ها نسبت به حالت خام اولیه شد و نمونه 3-10 کمترین نرخ خوردگی را داشت. نتایج آزمون امپدانس الکتروشیمیایی نیز با آزمون پلاریزاسیون تطابق داشته و افزایش مقاومت امپدانسی و افزایش مقاومت به خوردگی در نمونه‌های فراوری‌شده را تایید کرد. همچنین، ریزدانه‌شدن ساختار سطح و افزایش مساحت مرزدانه‌ها، علیرغم افزایش زبری، مقاومت به خوردگی را افزایش می‌دهد. عملیات سایش مکانیکی سطح باعث تشکیل لایه سخت‌شده‌ای شد که ضخامت آن با افزایش مدت‌زمان ساجمه‌زنی و کاهش قطر ساچمه بیشتر گردید و توزیع یکنواخت فازهای بین‌فلزی و ریزدانه شدن ساختار، خوردگی را از حالت موضعی به یکنواخت تغییر داد. این تغییرات در الگوهای پراش اشعه ایکس با کاهش شدت و افزایش پهنای پیک‌ها مشاهده شد.
کلیدواژه‌ها

عنوان مقاله English

Corrosion behavior investigation of 7075 aluminum alloy processed by surface mechanical attrition treatment

نویسندگان English

Mahmoud Ebrahimi
Reza Berjis
Department of Mechanical Engineering, Faculty of Engineering, University of Maragheh, Maragheh, Iran
چکیده English

Grain size, as a key structural parameter, plays a significant role in determining the mechanical and physical behavior of materials. In this regard, this research dealt with the effect of surface mechanical attrition treatment on the mechanical and corrosion behavior of 7075 aluminum alloy, which was investigated by varying the shot peening duration and shot size. The results showed that this process, in addition to refining the grain size from about 15 μm to less than 3 μm, significantly increased the hardness of the samples by up to 50%. Increasing the shot peening duration and decreasing the shot size led to further improvements in hardness, with the sample treated with 3 mm shots for 10 minutes (sample 3-10) exhibiting the highest hardness (72 Vickers). Moreover, surface mechanical attrition treatment reduced the corrosion rate of the samples compared to the as-received condition, with sample 3-10 showing the lowest corrosion rate. Electrochemical impedance spectroscopy results were consistent with polarization tests, confirming the enhancement of impedance and corrosion resistance in the processed samples. The Warburg parameter was identified as an indicator for evaluating the quality of the protective layer and ion diffusion. Additionally, grain refinement and increased grain boundary area, despite increased surface roughness, contributed to improved corrosion resistance. Also, the surface mechanical attrition treatment formed a harder outer layer that became thicker with longer peening durations and smaller shot sizes. Uniform distribution of intermetallic phases and grain refinement transformed the corrosion mode from localized to uniform. These changes were evident in X-ray diffraction patterns as decreased peak intensity and increased peak broadening.

کلیدواژه‌ها English

Severe Shot Peening
Ultrafine-Grained Materials
Hardness Test
Corrosion Resistance
[1]   Cabibbo M. Microstructure strengthening mechanisms in different equal channel angular pressed aluminum alloys. Materials Science and Engineering: A. 2013 Jan 10;560:413-32. doi: 10.1016/j.msea.2012.09.086
[2]   Morozova A, Kaibyshev R. Grain refinement and strengthening of a Cu–0.1 Cr–0.06 Zr alloy subjected to equal channel angular pressing. Philosophical Magazine. 2017 Aug 23;97(24):2053-76. doi: 10.1080/14786435.2017.1324649
[3]   Xun Y, Mohamed FA. Refining efficiency and capability of top-down synthesis of nanocrystalline materials. Materials Science and Engineering: A. 2011 Jun 25;528(16-17):5446-52. doi: 10.1016/j.msea.2011.03.015
[4]   Ebrahimi M, Shamsborhan M. Monotonic and dynamic mechanical properties of PTCAE aluminum. Journal of Alloys and Compounds. 2017 May 25;705:28-37. doi: 10.1016/j.jallcom.2017.02.109
[5]   Huppmann M, Lentz M, Chedid S, Reimers W. Analyses of deformation twinning in the extruded magnesium alloy AZ31 after compressive and cyclic loading. Journal of Materials Science. 2011 Feb;46(4):938-50. doi: 10.1007/s10853-010-4838-0
[6]   Guan RG, Tie D. A review on grain refinement of aluminum alloys: progresses, challenges and prospects. Acta Metallurgica Sinica (English Letters). 2017 May;30(5):409-32. doi: 10.1007/s40195-017-0565-8
[7]   Gode C, Attarilar S, Eghbali B, Ebrahimi M. Electrochemical behavior of equal channel angular pressed titanium for biomedical application. InAIP Conference Proceedings 2015 Mar 30 (Vol. 1653, No. 1, p. 020041). AIP Publishing LLC. doi: 10.1063/1.4914232
[8]   Peng K, Su L, Shaw LL, Qian KW. Grain refinement and crack prevention in constrained groove pressing of two-phase Cu–Zn alloys. Scripta Materialia. 2007 Jun 1;56(11):987-90. doi: 10.1016/j.scriptamat.2007.01.043
[9]   Figueiredo RB, Barbosa ER, Zhao X, Yang X, Liu X, Cetlin PR, Langdon TG. Improving the fatigue behavior of dental implants through processing commercial purity titanium by equal-channel angular pressing. Materials Science and Engineering: A. 2014 Dec 1;619:312-8. doi: 10.1016/j.msea.2014.09.099
[10] Xu C, Schroeder S, Berbon PB, Langdon TG. Principles of ECAP–Conform as a continuous process for achieving grain refinement: Application to an aluminum alloy. Acta Materialia. 2010 Feb 1;58(4):1379-86. doi: 10.1016/j.actamat.2009.10.044
[11] Cartigueyen S, Mahadevan K. Effects of heat input and particulate deposition on Cu/SiCp surface composite processed by friction stir processing. Indian J Eng Mater Sci (IJEMS). 2016 Apr 1;23(2&3):145-51.
[12] Swamy PK, Mylaraiah S, Gowdru Chandrashekarappa MP, Lakshmikanthan A, Pimenov DY, Giasin K, Krishna M. Corrosion behaviour of high-strength Al 7005 alloy and its composites reinforced with industrial waste-based fly ash and glass fibre: comparison of stir cast and extrusion conditions. Materials. 2021 Jul 14;14(14):3929. doi: 10.3390/ma14143929
[13] Bagheri S, Guagliano M. Review of shot peening processes to obtain nanocrystalline surfaces in metal alloys. Surface Engineering. 2009 Jan 1;25(1):3-14. doi: 10.1179/026708408X334087
[14] Djavanroodi F, Ebrahimi M, Rajabifar B, Akramizadeh S. Fatigue design factors for ECAPed materials. Materials Science and Engineering: A. 2010 Dec 15;528(2):745-50. doi: 10.1016/j.msea.2010.09.080
[15] Langdon TG. Twenty-five years of ultrafine-grained materials: Achieving exceptional properties through grain refinement. Acta Materialia. 2013 Nov 1;61(19):7035-59. doi: 10.1016/j.actamat.2013.08.018
[16] ATTARILAR S, SHAMSBORHAN M, EBRAHIMI M, GÖDE C, ÖZKAVAK HV. Enhancing mechanical properties and corrosion performance of AA6063 aluminum alloys through constrained groove pressing technique. Transactions of Nonferrous Metals Society of China. 2020 Jul 1;30(7):1790-802. doi: 10.1016/S1003-6326(20)65339-0
[17] Alipour Layin M, Ashrafi A, Khodadadi M. Experimental study of the flow forming process of grooved copper-aluminum bi-layer tubes and investigation of the separation force between the two layers. Iranian Journal of Manufacturing Engineering. 2025 Apr 21;12(2):44-58. doi: 10.22034/ijme.2025.498237.2040 [In Persian]
[18] Lapovok R, Estrin Y. Superplasticity in magnesium alloys by severe plastic deformation. InAdvances in Wrought Magnesium Alloys 2012 Jan 1 (pp. 144-185). Woodhead Publishing. doi: 10.1533/9780857093844.1.144
[19] Utyasheva FZ, Raabb GI, Zhilyaeva AP. Processing ultrafine-grained and nanostructured materials. In: Superplasticity and grain boundaries in ultrafine-grained materials. 2nd ed. Elsevier Ltd.; 2021 Jan. doi: 10.1016/B978-0-12-819063-0.00015-1
[20] Wan B, Chen W, Lu T, Liu F, Jiang Z, Mao M. Review of solid state recycling of aluminum chips. Resources, Conservation and Recycling. 2017 Oct 1;125:37-47. doi: 10.1016/j.resconrec.2017.06.004
[21] Ebrahimi M, Par MA. Twenty-year uninterrupted endeavor of friction stir processing by focusing on copper and its alloys. Journal of Alloys and Compounds. 2019 Apr 15;781:1074-90. doi: 10.1016/j.jallcom.2018.12.083
[22] Yu H, Tieu AK, Lu C, Liu X, Liu M, Godbole A, Kong C, Qin Q. A new insight into ductile fracture of ultrafine-grained Al-Mg alloys. Scientific Reports. 2015 Apr 8;5(1):9568. doi: 10.1038/srep09568
[23] Petryk H, Stupkiewicz S. A quantitative model of grain refinement and strain hardening during severe plastic deformation. Materials Science and Engineering: A. 2007 Jan 25;444(1-2):214-9. doi: 10.1016/j.msea.2006.08.076
[24] Gupta AK, Maddukuri TS, Singh SK. Constrained groove pressing for sheet metal processing. Progress in Materials Science. 2016 Dec 1;84:403-62. doi: 10.1016/j.pmatsci.2016.09.008
[25] Ostovari Moghaddam A, Mazinani A, Ketabchi M. Effect of accumulative roll bonding and equal channel angular rolling on microstructural and mechanical properties of Cu–Al–Mn shape memory alloys. Transactions of the Indian Institute of Metals. 2017 Sep;70(7):1901-9. doi: 10.1007/s12666-016-1007-4
[26] Fahimi Hanzaei A, Mousavi SM, Akbari J. Experimental and numerical study of environmental parameters' influence on the surface morphology of mesostructures fabricated by integrating additive manufacturing and electroforming processes. Iranian Journal of Manufacturing Engineering. 2025 Jan 20;11(11):15-25. doi: 10.22034/ijme.2024.477345.2006 [In Persian]
[27] Jafarzadeh H, Shalchi E, Shameli M. Fabrication and characterization of the mechanical properties of Al1050-CNT composites using accumulative channel-die compression bonding process. Iranian Journal of Manufacturing Engineering. 2024 Apr 20;11(2):69-81. doi: 10.22034/IJME.2024.437634.1922 [In Persian]
[28] Bagheri-Bami A, Honarpisheh M. An investigation of residual stress distribution in friction drilling of AA 7075 sheets by finite element modeling. Iranian Journal of Manufacturing Engineering. 2024 Apr 20;11(2):20-36. doi: 10.22034/IJME.2024.436544.1920 [In Persian]
[29] Horita Z, Fujinami T, Nemoto M, Langdon TG. Improvement of mechanical properties for Al alloys using equal-channel angular pressing. Journal of Materials Processing Technology. 2001 Nov 23;117(3):288-92. doi: 10.1016/S0924-0136(01)00783-X
[30] Beygelzimer Y, Varyukhin V, Synkov S, Orlov D. Useful properties of twist extrusion. Materials Science and Engineering: A. 2009 Mar 15;503(1-2):14-7. doi: 10.1016/j.msea.2007.12.055
[31] Cherukuri B, Nedkova TS, Srinivasan R. A comparison of the properties of SPD-processed AA-6061 by equal-channel angular pressing, multi-axial compressions/forgings and accumulative roll bonding. Materials Science and Engineering: A. 2005 Nov 25;410:394-7. doi: 10.1016/j.msea.2005.08.024
[32] Djavanroodi F, Ebrahimi M, Nayfeh JF. Tribological and mechanical investigation of multi-directional forged nickel. scientific reports. 2019 Jan 18;9(1):241. doi: 10.1038/s41598-018-36584-w
[33] Nadammal N, Kailas SV, Suwas S. A bottom-up approach for optimization of friction stir processing parameters; a study on aluminium 2024-T3 alloy. Materials & Design (1980-2015). 2015 Jan 1;65:127-38. doi: 10.1016/j.matdes.2014.09.005
[34] Attarilar S, Djavanroodi F, Ebrahimi M, Al-Fadhalah KJ, Wang L, Mozafari M. Hierarchical microstructure tailoring of pure titanium for enhancing cellular response at tissue-implant interface. Journal of Biomedical Nanotechnology. 2021 Jan 1;17(1):115-30. doi: 10.1166/jbn.2021.3015
[35] Hosseini S, Farajollahi M, Gode C, Ebrahimi M, Wang Q. Effect of surface condition on fatigue life of 7075 aluminium alloy. Canadian Metallurgical Quarterly. 2025 Oct 2;64(4):1875-85. doi: 10.1080/00084433.2024.2445969
[36] Antunes RA, De Oliveira MC. Effect of surface treatments on the fatigue life of magnesium and its alloys for biomedical applications. InSurface modification of magnesium and its alloys for biomedical applications 2015 Jan 1 (pp. 283-310). Woodhead Publishing. doi: 10.1016/B978-1-78242-077-4.00009-7
[37] Ravnikar D, Šturm R, Žagar S. Effect of shot peening on the strength and corrosion properties of 6082-T651 aluminium alloy. Materials. 2023 Jul 12;16(14):4976. doi: 10.3390/ma16144976
[38] Chen H, Yang J, Zhou HA, Moering J, Yin ZH, Gong Y, Zhao K. Mechanical properties of gradient structure Mg alloy. Metallurgical and Materials Transactions A. 2017 Sep;48(9):3961-70. doi: 10.1007/s11661-017-4216-5
[39] Attarilar S, Salehi MT, Al-Fadhalah KJ, Djavanroodi F, Mozafari M. Functionally graded titanium implants: Characteristic enhancement induced by combined severe plastic deformation. PLoS One. 2019 Aug 23;14(8):e0221491. doi: 10.1371/journal.pone.0221491
[40] Maleki E, Bagherifard S, Astaraee AH, Sgarbazzini S, Bandini M, Guagliano M. Application of gradient severe shot peening as a novel mechanical surface treatment on fatigue behavior of additively manufactured AlSi10Mg. Materials Science and Engineering: A. 2023 Aug 10;881:145397. doi: 10.1016/j.msea.2023.145397
[41] Shaeri MH, Shaeri M, Ebrahimi M, Salehi MT, Seyyedein SH. Effect of ECAP temperature on microstructure and mechanical properties of Al–Zn–Mg–Cu alloy. Progress in Natural Science: Materials International. 2016 Apr 1;26(2):182-91. doi: 10.1016/j.pnsc.2016.03.003
[42] Ebrahimi M, Gode C. Severely deformed copper by equal channel angular pressing. Progress in Natural Science: Materials International. 2017 Apr 1;27(2):244-50. doi: 10.1016/j.pnsc.2017.03.002
[43] Pandey V, Singh JK, Chattopadhyay K, Srinivas NS, Singh V. Influence of ultrasonic shot peening on corrosion behavior of 7075 aluminum alloy. Journal of Alloys and Compounds. 2017 Nov 5;723:826-40. doi: 10.1016/j.jallcom.2017.06.310
[44] Sun Q, Yang M, Jiang Y, Lei L, Zhang Y. Achieving excellent corrosion resistance properties of 7075 Al alloy via ultrasonic surface rolling treatment. Journal of Alloys and Compounds. 2022 Aug 5;911:165009. doi: 10.1016/j.jallcom.2022.165009
[45] Yazdani F, Rabiee SM, Jamaati R. Comparison of conventional and severe shot peening effects on the microstructure, texture, roughness, hardness, and electrochemical behavior of austenitic stainless steel. Heliyon. 2024 May 30;10(10). doi: 10.1016/j.heliyon.2024.e31284
[46] Edward AB, Heyns PS, Pietra F. Shot peening modeling and simulation for RCS assessment. Procedia Manufacturing. 2017 Jan 1;7:172-7. doi: 10.1016/j.promfg.2016.12.044
[47] Miková K, Bagherifard S, Bokuvka O, Guagliano M, Trško L. Fatigue behavior of X70 microalloyed steel after severe shot peening. International Journal of Fatigue. 2013 Oct 1;55:33-42. doi: 10.1016/j.ijfatigue.2013.04.021
[48] Ebrahimi M, Pashmforoush F, Gode C. Evaluating influence degree of equal-channel angular pressing parameters based on finite element analysis and response surface methodology. Journal of the Brazilian Society of Mechanical Sciences and Engineering. 2019 Feb;41(2):95. doi: 10.1007/s40430-019-1597-y
[49] Ebrahimi M. Numerical analysis of conventional and modified equal channel angular pressing. Transactions of the Indian Institute of Metals. 2019 Sep;72(9):2263-73. doi: 10.1007/s12666-019-01675-3
[50] Cao R, Yu X, Feng Z, Ojima M, Inoue J, Koseki T. Effect of annealing temperature and time on microstructure and mechanical properties of multilayered steel composite sheets. Metallurgical and Materials Transactions A. 2016 Dec;47(12):6042-55. doi: 10.1007/s11661-016-3747-5